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Chemical identification and genotoxicity analysis of petrochemical industrial wastewater

Jing ZHANG, Shigong WANG, Can WANG, Hongying HU

《环境科学与工程前沿（英文）》 2012年 第6卷 第3期   页码 350-359 doi: 10.1007/s11783-012-0404-0

摘要： The actual harmful effects of industrial wastewater can not be reflected by the conventional water quality index. Therefore, the change in dissolved organic matter and the genetic toxicity of petrochemical wastewater were observed in the current study by examining the wastewater treatment plant of a large petrochemical enterprise in Northwest China. Using XAD-8, MSC, and DA-7 resins, the wastewater was separated into six fractions, namely, hydrophobic acid (HOA), hydrophobic neutral (HOB), hydrophobic alkaline, hydrophilic acid, hydrophilic alkaline, and hydrophilic neutral. Umu-test was used to detect the genetic toxicity of the wastewater samples, and fluorescence spectra were also obtained to examine genetic toxic substances. The results show that wastewater treatment facilities can effectively reduce the concentration of organic matter in petrochemical wastewater ( <0.05). However, the mixing of aniline wastewater can increase the amount of organic carbon ( <0.05) and can overload facilities. This finding shows that the mixed collection and joint treatment of different types of petrochemical wastewater can affect the water quality of the effluent. Particularly, hydrophobic substances can be difficult to remove and account for a relatively large proportion of the effluent. The mixture of aniline wastewater can increase the genetic toxicity of the effluent ( <0.05), and biologic treatment can not effectively decrease the toxicity. Most of the genetic toxicology may exist in the HOA and HOB fractions. Fluorescence spectroscopy also confirms this result, and tryptophan-like substances may play an important role in genetic toxicity.

关键词： dissolved organic matter     resin fraction     genetic toxicity     fluorescence excitation and emission matrix    

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Control strategies for disinfection byproducts by ion exchange resin, nanofiltration and their sequential

《环境科学与工程前沿（英文）》 2023年 第17卷 第10期 doi: 10.1007/s11783-023-1725-x

摘要：

● Effects of AER adsorption and NF on DBP precursors, DBPs, and TOX were examined.

关键词： Disinfection byproducts     Control     Anion exchange resin     Nanofiltration     Cytotoxicity    

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Removal of dissolved oxygen from water using a Pd-resin based catalytic reactor

Wenxin SHI, Chongwei CUI, Liye ZHAO, Shuili YU, Xia YUN

《化学科学与工程前沿（英文）》 2009年 第3卷 第1期   页码 107-111 doi: 10.1007/s11705-009-0154-0

摘要： The removal of dissolved oxygen (DO) from water was studied experimentally in a Pd-resin base catalyst reactor using purified hydrogen gas as a reducing agent. The effects of various operating conditions, such as hydrogen and water flow rates, height of the catalytic resin bed, temperature, pH value and run time, on the removal of DO, had been studied extensively. The results shows that DO could be removed by the reactor from ppm to ppb levels at ambient temperature. Increases of temperature, H gas rate and the height of the catalytic resin were helpful to improve the DO removal rate. The change of pH value from 4 to 12 resulted in no effect on DO removal. Reaction time was the key factor to control the DO removal efficiency. Only when the reaction time was longer than 2.3 minutes under the experimental conditions, could a very low DO level be achieved.

关键词： dissolved oxygen     palladium     catalytic reactor     hydrogen     resin    

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Anti-hyperglycemic effect of the polysaccharide fraction isolated from mactra veneriformis

Lingchong WANG, Hao WU, Nian CHANG, Kun ZHANG

《化学科学与工程前沿（英文）》 2011年 第5卷 第2期   页码 238-244 doi: 10.1007/s11705-010-0002-2

摘要： Total macromolecule extract was obtained from the soft body of by the coupling techniques of decoction and alcohol precipitation. The extract was deproteinized with an ion exchange column, and resulted in the purifying of the crude polysaccharide fraction. It was found by chemical analysis that the crude polysaccharide part is composed of abundant polysaccharides (>95%) and few proteins (<1%). Furthermore, only one type of monosaccharide, glucose, was detected from its hydrolytes by thin-layer chromatography, indicating that the polysaccharides might be analogs of glucosan. The anti-hyperglycemia effects of the crude polysaccharide part were preliminarily investigated using several pharmacological methods in normal and diabetic mice. Animal experimental results showed that the crude polysaccharide fraction exhibited proper glycemia inhibition activity, and 300 mg/kg-weight dose has the optimal effect among all the studied doses. It is concluded that the crude polysaccharide fraction can be explored as a novel health product that possesses potential as an anti-hyperglycemic agent.

关键词： anti-hyperglycemia     Mactra veneriformis     polysaccharide     monosaccharide composition     oral glucose tolerance test    

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Impregnation of thermoplastic resin in jute fiber mat

LIU Xiaoye, DAI Gance

《化学科学与工程前沿（英文）》 2008年 第2卷 第2期   页码 145-149 doi: 10.1007/s11705-008-0030-3

摘要： Impregnation rate of thermoplastic resin (polypropylene) in jute fiber mat and influence of relative factors on impregnation were studied, aiming to develop the continuous melt impregnation technique and to investigate the effect of impregnation rate and temperature on processing conditions and mechanical properties of natural fiber mat-reinforced thermoplastics. Influence of pressure on porosity of fiber mat and effect of melt viscosity on impregnation rate were also investigated. The modified capillary rheometer was used as apparatus and experimental data were analyzed based on the one-dimension Darcy’s law. Results showed that at a given pressure, the impregnation rate is inversely proportional to melt viscosity and jute fiber mat has higher porosity than glass fiber mat. The architecture, compressibility, permeability and fiber diameter of jute fiber mat were compared with those of glass fiber mat and their effects on impregnation were discussed further. It could be seen that the average diameter of jute fiber is much bigger; the porosity of jute fiber mat is significantly higher and inner bundle impregnation does not exist in jute fiber mat. Therefore, it is not difficult to understand why the impregnation rate in jute fiber mat is 3.5 times higher and permeability is 14 times greater. Kozeny constants of jute and glass fiber mats calculated based on the capillary model are 2950 and 442, respectively.

关键词： polypropylene     diameter     influence     proportional     impregnation    

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FMO3--TMAO axis modulates the clinical outcome in chronic heart-failure patients with reduced ejection fraction

《医学前沿（英文）》 2022年 第16卷 第2期   页码 295-305 doi: 10.1007/s11684-021-0857-2

摘要： The association among plasma trimethylamine-N-oxide (TMAO), FMO3 polymorphisms, and chronic heart failure (CHF) remains to be elucidated. TMAO is a microbiota-dependent metabolite from dietary choline and carnitine. A prospective study was performed including 955 consecutively diagnosed CHF patients with reduced ejection fraction, with the longest follow-up of 7 years. The concentrations of plasma TMAO and its precursors, namely, choline and carnitine, were determined by liquid chromatography-mass spectrometry, and the FMO3 E158K polymorphisms (rs2266782) were genotyped. The top tertile of plasma TMAO was associated with a significant increment in hazard ratio (HR) for the composite outcome of cardiovascular death or heart transplantation (HR=1.47, 95% CI=1.13–1.91, P=0.004) compared with the lowest tertile. After adjustments of the potential confounders, higher TMAO could still be used to predict the risk of the primary endpoint (adjusted HR=1.33, 95% CI=1.01–1.74, P=0.039). This result was also obtained after further adjustment for carnitine (adjusted HR=1.33, 95% CI=1.01–1.74, P=0.039). The FMO3 rs2266782 polymorphism was associated with the plasma TMAO concentrations in our cohort, and lower TMAO levels were found in the AA-genotype. Thus, higher plasma TMAO levels indicated increased risk of the composite outcome of cardiovascular death or heart transplantation independent of potential confounders, and the FMO3 AA-genotype in rs2266782 was related to lower plasma TMAO levels.

关键词： chronic heart failure     trimethylamine-N-oxide     flavin monooxygenase 3     single nucleotide polymorphism    

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Effect of ignition timing and hydrogen fraction on combustion and emission characteristics of natural

WANG Jinhua, HUANG Zuohua, LIU Bing, ZENG Ke, YU Jinrong, JIANG Deming

《能源前沿（英文）》 2008年 第2卷 第2期   页码 194-201 doi: 10.1007/s11708-008-0035-0

摘要： An experimental study on the combustion and emission characteristics of a direct-injection spark-ignited engine fueled with natural gas/hydrogen blends under various ignition timings was conducted. The results show that ignition timing has a significant influence on engine performance, combustion and emissions. The interval between the end of fuel injection and ignition timing is a very important parameter for direct-injection natural gas engines. The turbulent flow in the combustion chamber generated by the fuel jet remains high and relative strong mixture stratification is introduced when decreasing the angle interval between the end of fuel injection and ignition timing giving fast burning rates and high thermal efficiencies. The maximum cylinder gas pressure, maximum mean gas temperature, maximum rate of pressure rise and maximum heat release rate increase with the advancing of ignition timing. However, these parameters do not vary much with hydrogen addition under specific ignition timing indicating that a small hydrogen fraction addition of less than 20% in the present experiment has little influence on combustion parameters under specific ignition timing. The exhaust HC emission decreases while the exhaust CO concentration increases with the advancing of ignition timing. In the lean combustion condition, the exhaust CO does not vary much with ignition timing. At the same ignition timing, the exhaust HC decreases with hydrogen addition while the exhaust CO and CO do not vary much with hydrogen addition. The exhaust NO increases with the advancing of ignition timing and the behavior tends to be more obvious at large ignition advance angle. The brake mean effective pressure and the effective thermal efficiency of natural gas/hydrogen mixture combustion increase compared with those of natural gas combustion when the hydrogen fraction is over 10%.
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Adsorption of 1,3-propanediol from synthetic mixture using polymeric resin as adsorbents

W. LUERRUK, A. SHOTIPRUK, V. TANTAYAKOM, P. PRASITCHOKE, C. MUANGNAPOH

《化学科学与工程前沿（英文）》 2009年 第3卷 第1期   页码 52-57 doi: 10.1007/s11705-009-0087-7

摘要： The aim of this work was to separate 1,3-PDO from a synthetic mixture using polymeric resins, Amberlite XAD-7 and XAD-16 resins. The equilibrium adsorption of 1,3-PDO onto two polymeric resins were investigated in binary and tertiary systems. Experimental results of binary component adsorption equilibrium indicated that the adsorption capacity ( ) of 1,3-PDO at 160 g/L onto XAD-7 and XAD-16 was 835.96 and 584.61 mg 1,3-PDO/g dry resin, respectively. The adsorption isotherms were closely predicted by the Langmuir-Freundlich model among the two isotherm model tested. The value of n of 1,3-PDO adsorbed on XAD-7 are much higher than those on XAD-16. This result suggested that XAD-7 resin has a higher affinity for the 1,3-PDO adsorption than XAD-16 resin. Moreover, the value of adsorption capacity of 1,3-PDO in the binary and tertiary component were compared at the same conditions. In the tertiary system, although the selectivity of 1,3-PDO from XAD-7 was approximately six times higher than XAD-16, the adsorption capacity of 1,3-PDO at 160 g/L onto XAD-16 was higher than XAD-7. Interestingly, the reusability of XAD-7 and XAD-16 resins in the three cycle times shows a slight loss of adsorption capacity. Furthermore, the investigation about desorption by an ethanol/water mixture at 50% ( / ) indicated that the desorption yield of 1,3-PDO from XAD-7 was lower than XAD-16 resin for both the binary and tertiary component. This was due to the more favorable adsorption characteristics of XAD-7 resin than XAD-16 resin.

关键词： adsorption     1     3-propanediol     glycerol     polymeric resin     adsorption isotherm    

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Comparison between two commercial uranium resins and a uranyl sulphate imprinted resin based on self-assembling

LIU Yaochi, XU Wei, XU Weijian, LIU Hanmao, ZHANG Xiaowen

《化学科学与工程前沿（英文）》 2007年 第1卷 第4期   页码 327-331 doi: 10.1007/s11705-007-0059-8

摘要： In recent years, resins prepared via molecular imprinting technology have received considerable attention owing to their recognition and selective adsorption. This paper deals with the comparative investigation between a uranyl sulphate imprinted ion-exchange based on self-assembling molecular imprinting technology and two kinds of commercial uranium resins (the medium pore resin D263 and strong base resin 201×7). The studies were focused on their kinetics performance, adaptability toward pH, and performance of saturation and elution in laboratory-scale column. The results show that the imprinted ion exchange resin has the fast kinetics, high adaptability toward pH, and good adsorption and elution performance.

关键词： saturation     molecular imprinting     imprinting technology     adaptability     commercial    

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Performance of steel bridge deck pavement structure with ultra high performance concrete based on resin

《结构与土木工程前沿（英文）》 2021年 第15卷 第4期   页码 895-904 doi: 10.1007/s11709-021-0759-z

摘要： This research investigated a pavement system on steel bridge decks that use epoxy resin (EP) bonded ultra-high performance concrete (UHPC). Through FEM analysis and static and dynamic bending fatigue tests of the composite structure, the influences of the interface of the pavement layer, reinforcement, and different paving materials on the structural performance were compared and analyzed. The results show that the resin bonded UHPC pavement structure can reduce the weld strain in the steel plate by about 32% and the relative deflection between ribs by about 52% under standard axial load conditions compared to traditional pavements. The EP bonding layer can nearly double the drawing strength of the pavement interface from 1.3 MPa, and improve the bending resistance of the UHPC structure on steel bridge decks by about 50%; the bending resistance of reinforced UHPC structures is twice that of unreinforced UHPC structure, and the dynamic deflection of the UHPC pavement structure increases exponentially with increasing fatigue load. The fatigue life is about 1.2 × 107 cycles under a fixed force of 9 kN and a dynamic deflection of 0.35 mm, which meets the requirements for fatigue performance of pavements on steel bridge decks under traffic conditions of large flow and heavy load.

关键词： steel bridge deck pavement     ultra-high-performance concrete     epoxy resin     composite structure     bending fatigue performance    

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Self-extinguishing and transparent epoxy resin modified by a phosphine oxide-containing bio-based derivative

Gang Tang, Ruiqing Zhao, Dan Deng, Yadong Yang, Depeng Chen, Bing Zhang, Xinliang Liu, Xiuyu Liu

《化学科学与工程前沿（英文）》 2021年 第15卷 第5期   页码 1269-1280 doi: 10.1007/s11705-021-2042-1

摘要： A phosphine oxide-containing bio-based curing agent was synthesized by addition reaction between furan derivatives and diphenylphosphine oxide. The molecular structure of the as-prepared bio-based curing agent was confirmed by Fourier transform infrared spectroscopy and nuclear magnetic resonance spectroscopy. Dynamic mechanical analysis results indicated that with the increase of bio-based curing agent content, the glass transition temperature of epoxy/bio-based curing agent composites decreased, which was related to the steric effect of diphenylphosphine oxide species that possibly hinder the curing reaction as well as the reduction in the cross-linking density by mono-functional N H. By the addition of 7.5 wt-% bio-based curing agent, the resulting epoxy composite achieved UL-94 V-0 rating, in addition to limiting oxygen index of 32.0 vol-%. With the increase of content for the bio-based curing agent, the peak of heat release rate and total heat release of the composites gradually decreased. The bio-based curing agent promoted the carbonization of the epoxy matrix, leading to higher char yield with good thermal resistance. The high-quality char layer served as an effective barrier to retard the diffusion of decomposition volatiles and oxygen between molten polymers and the flame. This study provides a renewable strategy for fabricating flame retardant and transparent epoxy thermoset.

关键词： epoxy resin     flame retardant     furan derivative     diphenylphosphine oxide    

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Condensation of phenol and acetone on a modified macroreticular ion exchange resin catalyst

Baohe WANG, Lili WANG, Jing ZHU, Shuang CHEN, Hao SUN

《化学科学与工程前沿（英文）》 2013年 第7卷 第2期   页码 218-225 doi: 10.1007/s11705-013-1330-9

摘要： Macroreticular ion exchange resin catalysts were prepared by suspension polymerization, and then modified by alkylmercaptoamines. The modified catalysts were characterized by N adsorption/desorption measurements, scanning electron microscopy and differential scanning calorimetry. Key factors such as the mercaptan content, the degree of crosslinking and the structures of the promoters were investigated for the synthesis of Bisphenol A (BPA). At optimal conditions, the macroreticular ion exchange resin catalysts modified by alkylmercaptoamines showed high catalytic activity and selectivity for BPA synthesis.

关键词： macroreticular ion exchange resin     catalysts     suspension polymerization     Bisphenol A    

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Utilization of nano/micro-size iron recovered from the fine fraction of automobile shredder residue for

Jiwan SINGH, Yoon-Young CHANG, Jae-Kyu YANG, Seon-Hong KANG, Janardhan Reddy KODURU

《环境科学与工程前沿（英文）》 2016年 第10卷 第4期 doi: 10.1007/s11783-016-0848-8

摘要： Phenol removal by n/m Fe in the presence of H O was highly effective. Increasing the amounts of n/m Fe and H O ?increased the phenol removal rate. Phenol removal was decreased with an increase in the concentration of phenol. The natural pH (6.9) of the solution was highly effective for phenol removal. The pseudo-first-order kinetics was best fitted for the degradation of phenol. The study investigates the magnetic separation of Fe from automobile shredder residue (ASR) (<0.25 mm) and its application for phenol degradation in water. The magnetically separated Fe was subjected to an ultrasonically assisted acid treatment, and the degradation of phenol in an aqueous solution using nano/micro-size Fe (n/m Fe) was investigated in an effort to evaluate the possibility of utilizing n/m Fe to remove phenol from wastewater. The prepared n/m Fe was analyzed by scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR). The effects of the dosages of n/mFe, pH, concentration of phenol and amount of H O on phenol removal were evaluated. The results confirm that the phenol degradation rate was improved with an increase in the dosages of n/mFe and H O ; however, the rate is reduced when the phenol concentration is higher. The degradation of phenol by n/mFe followed the pseudo-first-order kinetics. The value of the reaction rate constant ( was increased as the amounts of n/m Fe and H O increased. Conversely, the value of was reduced when the concentration of phenol was increased. The probable mechanism behind the degradation of phenol by n/m Fe is the oxidation of phenol through hydroxyl radicals which are produced during the reaction between H O and n/m Fe.

关键词： Automobile shredder residue (ASR)     Fe     Phenol     Scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR)     Mechanism    

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Emission characteristics of a turbocharged diesel engine fueled with gas-to-liquids

WU Tao, ZHANG Wugao, FANG Junhua, HUANG Zhen

《能源前沿（英文）》 2007年 第1卷 第3期   页码 331-335 doi: 10.1007/s11708-007-0049-z

摘要： Emission characteristics of a turbocharged, inter-cooled, heavy-duty diesel engine operating on neat gas-to-liquids (GTL) and blends of GTL with conventional diesel were investigated and a comparison was made with those of diesel fuel. The results show that nitrogen oxides (NO), smoke, and particulate matter (PM) emissions can be decreased when operating on GTL and diesel-GTL blends. Engine emissions decrease with an increase of GTL fraction in the blends. Compared with diesel fuel, an engine operating on GTL can reduce NO, PM, carbon monoxide (CO), and hydrocarbon (HC) by 23.7%, 27.6%, 16.6% and 12.9% in ECE R49 13-mode procedure, respectively. Engine speed and load have great influences on emissions when operating on diesel-GTL blends and diesel fuel in the turbocharged diesel engine. The study indicates that GTL is a promising alternative fuel for diesel engines to reduce emissions.

关键词： comparison     conventional     fraction     13-mode procedure     study    

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Exceptionally flame-retardant flexible polyurethane foam composites: synergistic effect of the silicone resin

Qian Wu, Jincheng Zhang, Shengpeng Wang, Bajin Chen, Yijun Feng, Yongbing Pei, Yue Yan, Longcheng Tang, Huayu Qiu, Lianbin Wu

《化学科学与工程前沿（英文）》 2021年 第15卷 第4期   页码 969-983 doi: 10.1007/s11705-020-1988-8

摘要： A facile strategy was developed to fabricate flexible polyurethane (PU) foam composites with exceptional flame retardancy. The approach involves the incorporation of graphene oxide (GO) into a silicone resin (SiR) solution, which is then deposited onto a PU foam surface via the dip-coating technique and cured. Fourier-transform infrared spectroscopy, scanning electron microscopy, and Raman spectroscopy measurements demonstrated that the SiR and GO were successfully coated onto the PU skeleton and the intrinsic porous structure of the PU foam remained intact. The effects of SiR and GO on the mechanical and thermal stability and flame retardancy of PU composites were evaluated through compression tests, thermogravimetric analysis, vertical combustion tests, and the limiting oxygen index. The measurement results revealed that the composites (PU@SiR-GO) showed superior flame retardancy and thermal and mechanical stability compared to pristine PU or PU coated with SiR alone. The mechanical and thermal stability and the flame-retardant properties of the PU composites were enhanced significantly with increasing GO content. Based on the composition, microstructure, and surface morphology of PU@SiR-GO composites before and after combustion tests, a possible flame-retardance mechanism is proposed. This work provides a simple and effective strategy for fabricating flame-retardant composites with improved mechanical performance.

关键词： flame retardancy     flexible polyurethane foam     graphene oxide     silicone resin    

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标题 作者 时间 类型 操作

Chemical identification and genotoxicity analysis of petrochemical industrial wastewater

Jing ZHANG, Shigong WANG, Can WANG, Hongying HU

期刊论文

Control strategies for disinfection byproducts by ion exchange resin, nanofiltration and their sequential

期刊论文

Removal of dissolved oxygen from water using a Pd-resin based catalytic reactor

Wenxin SHI, Chongwei CUI, Liye ZHAO, Shuili YU, Xia YUN

期刊论文

Anti-hyperglycemic effect of the polysaccharide fraction isolated from mactra veneriformis

Lingchong WANG, Hao WU, Nian CHANG, Kun ZHANG

期刊论文

Impregnation of thermoplastic resin in jute fiber mat

LIU Xiaoye, DAI Gance

期刊论文

FMO3--TMAO axis modulates the clinical outcome in chronic heart-failure patients with reduced ejection fraction

期刊论文

Effect of ignition timing and hydrogen fraction on combustion and emission characteristics of natural

WANG Jinhua, HUANG Zuohua, LIU Bing, ZENG Ke, YU Jinrong, JIANG Deming

期刊论文

Adsorption of 1,3-propanediol from synthetic mixture using polymeric resin as adsorbents

W. LUERRUK, A. SHOTIPRUK, V. TANTAYAKOM, P. PRASITCHOKE, C. MUANGNAPOH

期刊论文

Comparison between two commercial uranium resins and a uranyl sulphate imprinted resin based on self-assembling

LIU Yaochi, XU Wei, XU Weijian, LIU Hanmao, ZHANG Xiaowen

期刊论文

Performance of steel bridge deck pavement structure with ultra high performance concrete based on resin

期刊论文

Self-extinguishing and transparent epoxy resin modified by a phosphine oxide-containing bio-based derivative

Gang Tang, Ruiqing Zhao, Dan Deng, Yadong Yang, Depeng Chen, Bing Zhang, Xinliang Liu, Xiuyu Liu

期刊论文

Condensation of phenol and acetone on a modified macroreticular ion exchange resin catalyst

Baohe WANG, Lili WANG, Jing ZHU, Shuang CHEN, Hao SUN

期刊论文

Utilization of nano/micro-size iron recovered from the fine fraction of automobile shredder residue for

Jiwan SINGH, Yoon-Young CHANG, Jae-Kyu YANG, Seon-Hong KANG, Janardhan Reddy KODURU

期刊论文

Emission characteristics of a turbocharged diesel engine fueled with gas-to-liquids

WU Tao, ZHANG Wugao, FANG Junhua, HUANG Zhen

期刊论文

Exceptionally flame-retardant flexible polyurethane foam composites: synergistic effect of the silicone resin

Qian Wu, Jincheng Zhang, Shengpeng Wang, Bajin Chen, Yijun Feng, Yongbing Pei, Yue Yan, Longcheng Tang, Huayu Qiu, Lianbin Wu

期刊论文